This instruction has been written for a supervised session performed in a chemical lab. Be careful when applying to a different environment.

In the first lab you designed a PCB from a given circuit in EAGLE. This lab is about producing the printed circuit board from that design. There are two major techniques for PCB manufacturing. For prototyping purposes it is popular to use a special milling machine for PCBs. The faculty uses a LPKF ProtoMat S62 in its electronics workshop. The EAGLE board design is exported to gerber and excellon files and after making some adjustments in a CAM tool like CircuitCAM the design can be used for milling out copper-clad boards. The machine isolates all traces on the board and drills holes where necessary.

The technique we will cover today employs a chemical process to create PCBs. To put it simply it is a four step procedure:

1. prepare development and etching solutions
2. expose board to uv light while protecting certain areas with a mask
3. develop board using sodium hydroxide
4. etch board using sodium persulfate

This process is widely used in industry for producing PCBs.

At the end of today's experiment each student will have his/her own layout etched to a board.

Magnetrührer, Waage, Spatel, Glasrührstab, Becherglas 2l, 500ml, Becherglas für 300g, Thermometer, Ethanol, Papiertücher, Torx-Schraubendreher, Tacker, Scheren ruler, scissors, plate shear, chemistry lab, sink, fume extractor, safety goggles, lab coat, gloves, printer, transparent foil, uv exposer devices, fotosensitive base material, development and etching solution, containers, etching bath, aceton, Wattepads, Lötlack

Please read the chemistry lab safety rules on Moodle before taking the experiment. The safety rules will also be pointed out at the beginning of the experiment.

We will work with the following substances in this lab:

• toner compressor
• Developer / sodium hydroxide (Natriumhydroxid, NaOH)
• Etchant / sodium persulafte (Natriumpersulfat, Na₂S₂O₈)
• item ethanol (C₂H₆O)
• item distilled (purified) water (H₂O)

Get your safety equipment. This includes glasses, lab coat and gloves. Make yourself familiar with the provided tools.

1. Make sure you have a bowl like shown in figure 1. It will be used as container for the development solution. You should also have a 500 ml beaker (see figure 2) for measurement, a glass rod for stirring and a weighing boat.
2. Fill the beaker with 250 ml distilled water.
3. Get 5g sodium hydroxide from the front of the classroom and fill it into your beaker. In order to get the right amount use the precision scale and a weighing boat. Close the container of sodium hydroxide as sodium hydroxide is hrydrophilic.
4. Stir the liquid in the beaker with a glass rod until everything is dissolved.
5. Pour the solution into the plastic bowl.
6. Make sure you have a big glass beaker like shown in figure 2, a magnetic stirrer (see figure 3), a thermometer and a small beaker with sodium persulfate.
7. Fill the big beaker with approximately 1.6 liter of distilled water.
8. Add 300g sodium persulfate to it, it should be already prepared in the second beaker.
9. Use the magnetic stirrer to heat the big beaker up and help dissolving the sodium persulfate at the same time (setting 4 / 4). As etching etching works best above 40°C (and below 50°C). Try to heat the solution up until it reaches 40°C.
10. When the solution is ready turn off the magnetic stirrer and pour the solution carefully into the etching device.
11. Turn on the heating and air compressor of the etching device by plugging it into the electric outlets.

Fig. 1: Bowl Fig. 2: Beaker Fig. 3: Magnetic stirrer

1. Get the transparent foils containing your PCB design.
2. Go to the fume cupboard at the end of the room and apply some density spray to both foils. Make sure to apply it on the side with the printing.
3. Wait for it to dry. The black areas should be clearly darker now.
4. Use the scissors to cut out your design. Leave a big surrounding area, as you will nedd it for stapeling.
5. Place the foils on top of each other. The sides with the printing on it have to be facing each other (the board will be in between of the foils later).
6. Staple the foils together while trying to align them perfectly.
7. Check the alignment. Misalignments will probably result in defective PCBs later.
8. Get a piece of fotensensitive base material (FR4 in this case) for exposure. It will be slightly bigger than your design so you should have no problems with that.
9. Remove the blue protection foil (see figure 4) on both sides.
10. Avoid exposing the unprotected plate to sunlight (all UV sources).
11. Put the copper plate between the transparent foils and put both under the glass plate of the uv exposure device (see figure 5, figure 6).
12. Beware: For your own safety avoid looking into the uv lights. The device is to be only turned on when closed!
13. Turn it on and wait for the vacuum to go up to 0.3, compare to figure 7. The vacuum prevents things from moving.
14. Set the exposure time to two minutes and thirty seconds (the display should read 2-3-0), make sure the bottom lights are also enabled as you are making a two sided PCB and start the device by pressing the knob once.
15. When the time is up the lights will automatically be turned off and the vacuum will be released.
16. Open the device and get out the exposed board.

Fig. 4: Remove protection foil Fig. 5: UV exposure device Fig. 6: Board under plate Fig. 7: Check vacuum

1. Remove the exposed board from the foils.
2. Put the board into the prepared bowl of the development solution. Stir it with a stick.
3. Brown residues from the exposed parts of the board should start to appear after a couple of seconds. Stir until the process seems to stop and take it out immediately. Do not leave the board in for longer than 90 seconds maximum.
4. Rinse the board thoroughly with (purified) water.
5. Check the temperature of the etching solution, it should be above 40 and below 50 degrees C.
6. Mount the board to the grey retainer (see figure 8). To speed up the procution process mount two boards at the same time.
7. Submerge the board(s) in the tank.
8. Wait for the etching process to complete. You may have to wait a couple of minutes before something seems to be happening but from this point it should be going quite fast and obvious.
9. Take out the board when etching is complete. Do not wait to long as it will affect the protected traces as well if you wait too long.
10. Rinse the board(s) thoroughly with (purified) water.
11. Repeat these steps until all team members have a PCB.
12. Shut down pump and heating.
13. Use ethanol and paper tissue to remove the remaining photoresist from the board(s). Be thorough.
14. Let the board(s) dry.
15. Clean the lab equipment. Ask the instructors on how to do that.

Fig. 8: Holder